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Department of Chemical and Metallurgical Engineering

Chemical Engineering in Aqueous Systems

The group, led by Prof. Marjatta Louhi-Kultanen, is studying the unit operations of aqueous systems and the solid-liquid phases equilibria.
Water has an important role in many unit operations in applications of the chemical industry, hydrometallurgy, wood processing, food production, the metal industry and biorefining. For instance, different types of unit operations of water systems include precipitation, crystallization, freezing, eutectic freeze crystallization, drying, evaporation, absorption and adsorption, dissolution, heat transfer and post-processing of liquids and solids.
For a deeper understanding and modelling of production processes, it is also important to know the states of equilibrium between multiphase systems. The gas-liquid, liquid-liquid, and solid-liquid states of equilibrium in water systems need to be known with a sufficient degree of precision.
Sea water

Recent research activities:

  1. Separation and purification of valued compounds from biorefineries, metals from waste and side streams, nutrients and other recyclable materials by crystallization and precipitation.
  2. Identification of critical impurities and their separation from solutions.
  3. Crystallization of mesocrystals for pharmaceutical applications.
  4. Regeneration of chemicals: concentration of aqueous solutions containing green solvents by freezing.
  5. Pre-treatment of aqueous electrolyte solutions to remove fine particles by microfiltration and organic compounds by adsorption containing.
  6. Real-time monitoring of crystal growth and nucleation kinetics and separation efficiency of microfiltration.

Our activities in images:

CHEM_Aqeous systems_Mesocrystals
CFD
CMET_Aqueous systems_Crystallization

Heat transfer in melt crystallizer (CFD simulation)

CFD
CMET_Aqueous systems_Crystallization
CHEM_Acqeous systems_setup for continuous process

Melt crystallization

CMET_Aqueous systems_Crystallization
CHEM_Acqeous systems_setup for continuous process
CHEM_Aqeous systems_Mesocrystals

Setup for continuous process

CHEM_Acqeous systems_setup for continuous process
CHEM_Aqeous systems_Mesocrystals
CFD

Mesocrystals

CHEM_Aqueous systems_student at lab
CHEM_Aqueous systems_student at lab

Our lab and facilities:

  • We have good facilities consisting of a laboratory scale stirred tank station which allows studies on continuous, semi-batch and batch process mode at ambient or lower pressures. The station is equipped with a calorimeter and accurate temperature control system. Various crystallization methods, such as cooling crystallization, evaporative crystallization, reactive crystallization and anti-solvent crystallization, can be investigated.
  • Melt crystallization devices for layer and suspension crystallization studies.
  • Solid-liquid equilibria research based on thermal analysis methods, solubility measurements and optical detection of saturation point of solutions.
  • Realtime monitoring of chord lengths of particulates in fluids.
  • Thermodynamic modeling of electrolyte and non-electrolyte solutions.
  • Vacuum and pressure test filters for filterability studies to determine principle filtration parameters.

Our Lab:

CHEM_aqueous systems_Easymax workstation
CMET_aqueous systems_boiling point
CHEM_aqueous systems_Lab_Easymax system

Image of boiling-point experimental setup: (1) vacuum pump, (2) condenser, (3) pressure gauge, (4) thermometer, (5) magnetic stirrer, (6) heating mantle.

CMET_aqueous systems_boiling point
CHEM_aqueous systems_Lab_Easymax system
CHEM_aqueous systems_Easymax workstation

EasyMax 402 crystallization system: (1, 2) reactors, (3) Focused Beam Reflectance Measurement tool, (4,4*) stirrers, (5) vacuum system, (6) control panel, (7) pump head, (8) digital drive.

CHEM_aqueous systems_Lab_Easymax system
CHEM_aqueous systems_Easymax workstation
CMET_aqueous systems_boiling point

EasyMax workstation

Our research group members:

CHEM_Jianxin Zhang at the lab
CHEM_Aqueous Systems_research group members
CHEM_Anna Zaykovskaya at the lab

Our team (from left to right): Anna, Nahla, Marjatta, Mitra, Jianxin and Rajaboopathi.

CHEM_Aqueous Systems_research group members
CHEM_Anna Zaykovskaya at the lab
CHEM_Nahla Osmanbegovic at the lab

Anna at the lab.

CHEM_Anna Zaykovskaya at the lab
CHEM_Nahla Osmanbegovic at the lab
CHEM_Jianxin Zhang at the lab

Mitra at the lab.

CHEM_Nahla Osmanbegovic at the lab
CHEM_Jianxin Zhang at the lab
CHEM_Aqueous Systems_research group members

Jianxin at the lab.

Latest publications:

Paula Översti, Bing Han, Eeva-Leena Rautama, Jari Kavakka, Staffan Torssell, Pekka Oinas, Marjatta Louhi-Kultanen 2026 Crystal Growth and Design

Anna Zaykovskaya, Mitra Ila, Michael Ginter, Erik Temmel, Martin Schwiderski, Manfred Stepanski, Marjatta Louhi-Kultanen 2026 Chemical Engineering and Technology

Bernadeth Amano, Marjatta Louhi-Kultanen 2025 Crystal Growth and Design

Mitra Ila, Paula Nousiainen, Donya Kamravamanesh, Tero Eerikäinen, Marjatta Louhi-Kultanen 2025 Chemical Engineering Journal

Paula Översti, Bing Han, Jari Kavakka, Staffan Torssell, Esko Tirronen, Marjatta Louhi-Kultanen, Pekka Oinas 2025 European Journal of Pharmaceutical Sciences

Paula Översti, Bing Han, Jari Kavakka, Staffan Torssell, Esko Tirronen, Marjatta Louhi-Kultanen, Pekka Oinas 2025 European Journal of Pharmaceutical Sciences

Mitra Ila, Kim Miikki, Marjatta Louhi-Kultanen 2024 Crystal Growth and Design

Anna Zaykovskaya 2024

Anna Zaykovskaya, Bernadeth Amano, Marjatta Louhi-Kultanen 2024 Crystal Growth and Design

Jianxin Zhang, Rajaboopathi Mani, Marjatta Louhi-Kultanen 2024 Hydrometallurgy
More information on our research in the Aalto research portal.
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